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*Correspondence: Ying Chen, [email protected] This article was submitted to Nutritional Immunology, a section of the journal Frontiers in Nutrition Disclaimer All claims expressed in this article are solely those of the authors and do not necessarily represent those of their affiliated organizations, or those of the publisher, the editors and the reviewers

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Pure HSP displayed a sharp melting peak and distinct diffraction pattern due to the crystalline nature of the drug

mobile phase B: acetonitrile with 0.1% formic acid

Using sterile supplies, adding BAC water slowly, avoiding unnecessary agitation, documenting reconstitution volumes, and storing peptides correctly will help support reproducible laboratory research