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Synthesis of ( R )-1D228 (1) Preparation of the intermediate 3 : an aqueous solution of sodium carbonate (sodium carbonate 13.2 mmol, 1.35 g, 6.5 mL water) was added into a solution of 5-fluoro-2-chloropyrimidine (6.6 mmol, 0.87 g) in toluene (13 mL), into which were then added bis(triphenyl phosphine)palladium chloride (1.36 mmol, 0.096 g), acetyl phenyl boronic acid (6.5 mmol, 1.05 g), and ethanol (6.5 mL)