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Although the reaction of PhSeBr and 1a generating the SeN intermediate INT1-Se is endothermic by 12.6 kcal mol 1 , INT1-Se may readily undergo a Se-centred [2,3]-sigmatropic rearrangement to generate an ortho -Se = N substituted dearomatized species ( INT2-Se ) via TS1-Se , with a barrier of 12.7 kcal mol 1

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Briefly, samples were mixed with 100 L methanol in the test tubes with a vortex mixer for 3-6 s, then 900 L FOX reaction mixtures (25 mM H 2 SO4, 100 M xylenol orange, 250 M FeSO4, and 4 mM BHT in 90% (v/v) methanol) was added and incubated for 30 min at room temperature