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Detection was performed on a Sciex 6500+ ESI-tripleQ MS/MS (AB Sciex Germany GmbH, Darmstadt, Germany) on low mass mode (01000 Da) with instrument settings as described in our previous work [40]

Nature 392:605608 Martin ER, Scott WK, Nance MA, Watts RL, Hubble JP, Koller WC, Lyons K, Pahwa R, Stern MB, Colcher A, et al (2001) Association of single-nucleotide polymorphisms of the tau gene with late-onset Parkinson disease

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Another aspect of the invention pertains to treating obesity or related chronic metabolic condition by administering a therapeutically effective amount of one or more cations of the invention followed by administration of one or more cations chosen from Tables 3a and 3b